对甲氧羰基苯硼酸频哪醇酯合成路线 (共 33 条)
反应条件
C37H51ClFeNPPd; potassium acetate in 1,4-dioxane T=80°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Lu, Jie; Guan, Zhong-Zhi; Gao, Jian-Wu; Zhang, Zhan-Hui
Applied Organometallic Chemistry, 2011 , vol. 25, # 7 p. 537 - 541
反应条件
NiCl2(PMe3)2; TMSOCH2CF3; cesium fluoride in tetrahydrofuran T=100°C; 12 h; Inert atmosphere;
参考文献
Yamamoto, Tetsuya; Morita, Tomoyuki; Takagi, Jun; Yamakawa, Tetsu
Organic Letters, 2011 , vol. 13, # 21 p. 5766 - 5769
反应条件
triethylamine; Pd(dppf)Cl2 in 1,4-dioxane
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane T=80°C; 21 h;
参考文献
Ishiyama, Tatsuo; Itoh, Yoshiya; Kitano, Takahiro; Miyaura, Norio
Tetrahedron Letters, 1997 , vol. 38, # 19 p. 3447 - 3450
反应条件
copper(l) iodide; palladium diacetate; caesium carbonate; triphenylphosphine in acetonitrile T=20°C; Miyaura Borylation Reaction; 24 h; chemoselective reaction;
参考文献
Ratniyom, Jadsada; Dechnarong, Nattanee; Yotphan, Sirilata; Kiatisevi, Supavadee
European Journal of Organic Chemistry, 2014 , vol. 2014, # 7 p. 1381 - 1385
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); 1,3-bis-(diphenylphosphino)propane; triethylamine in toluene T=100°C; 18 h; Inert atmosphere;
参考文献
Rosen, Brad M.; Huang, Chenghong; Percec, Virgil
Organic Letters, 2008 , vol. 10, # 12 p. 2597 - 2600
反应条件
copper(l) iodide; tributyl-amine in tetrahydrofuran T=20°C;
参考文献
Angewandte Chemie, International Edition, , vol. 48, p. 5350 - 5354
Angewandte Chemie, , vol. 121, p. 5454 - 5458
反应条件
1: p-bromophenyl bromide; 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 0.5 h; 2: With tert.-butyl lithium in tetrahydrofuran; pentane T=-78°C; 0.333333 h; 3: methoxycarbonyl cyanide in tetrahydrofuran; pentane T=-78 - 20°C; 1 h; Further stages.;
参考文献
Jiang, Qin; Ryan, Meagan; Zhichkin, Paul
Journal of Organic Chemistry, 2007 , vol. 72, # 17 p. 6618 - 6620
反应条件
in tetrahydrofuran T=20°C;
参考文献
Chemical Communications, , # 35 p. 3667 - 3669
反应条件
3-chloroprop-1-ene; trifluoroacetic acid; cobalt(II) dibromide in acetonitrile Zn dust (1.5 equiv., acid-activated) , CoBr2 (0.1 equiv.), stirred for 5min with allyl chloride (0.3 equiv.), a soln. of aryl halide (1 equiv.) and a soln. 1 equiv. of B compd. added at room temp., stirred for 30 mi n, tranesterificated with pinacol; hydrolized (NH4Cl), extd. (diethyl ether);
参考文献
Claudel, Stephanie; Gosmini, Corinne; Paris, Jean Marc; Perichon, Jacques
Chemical Communications, 2007 , # 35 p. 3667 - 3669