1-(对甲氧基苯基)2-硝基丙烯合成路线 (共 27 条)
反应条件
ammonium acetate T=90°C; Henry reaction; 0.416667 h; Microwave irradiation;
参考文献
Rodriguez, Jose M.; Dolors Pujol
Tetrahedron Letters, 2011 , vol. 52, # 21 p. 2629 - 2632
反应条件
ammonium acetate Henry reaction; Reflux;
参考文献
Munoz, Lourdes; Rodriguez, Anna M.; Rosell, Gloria; Bosch, M. Pilar; Guerrero, Angel
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8171 - 8177
反应条件
4-(N,N-dimethlyamino)pyridine in dichloromethane 0.5 h;
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
1: DMAP / diethyl ether / 5 h 2: 88 percent / DMAP / CH2Cl2 / 0.5 h View Scheme
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
1: 82 percent / t-BuOK / 2-methyl-propan-2-ol; tetrahydrofuran 2: DMAP / diethyl ether / 5 h 3: 88 percent / DMAP / CH2Cl2 / 0.5 h View Scheme
参考文献
Denmark, Scott E.; Kesler, Brenda S.; Moon, Young-Choon
Journal of Organic Chemistry, 1992 , vol. 57, # 18 p. 4912 - 4924
反应条件
pyridine; diethyl ether T=0°C;
参考文献
Allsop; Kenner
Journal of the Chemical Society, 1923 , vol. 123, p. 2314
参考文献
Schmidt; Fischer
Chemische Berichte, 1920 , vol. 53, p. 1539
反应条件
in acetonitrile T=30°C; var. temp.; Equilibrium constant;
参考文献
Shunmugasundaram, A; Thanulingam, T Lekshmana; Murugesan, R
Indian Journal of Chemistry, Section A: Inorganic, Bio-inorganic, Physical, Theoretical & Analytical Chemistry, 1991 , vol. 30, # 7 p. 609 - 613
反应条件
T=0°C; anschliessend Behandeln mit verd. Kalilauge;
参考文献
Allsop; Kenner
Journal of the Chemical Society, 1923 , vol. 123, p. 2314
参考文献
Schmidt; Fischer
Chemische Berichte, 1920 , vol. 53, p. 1539