1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.166667 h; Inert atmosphere;
2: diethyl chlorophosphate in tetrahydrofuran; hexane
1 h;
参考文献
Ha, Young-Geun; Emery, Jonathan D.; Bedzyk, Michael J.; Usta, Hakan; Facchetti, Antonio; Marks, Tobin J.
Journal of the American Chemical Society, 2011 , vol. 133, # 26 p. 10239 - 10250
CAN in acetonitrile
5 h; Ambient temperature; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kottmann, Hariolf; Skarzewski, Jacek; Effenberger, Franz
Synthesis, 1987 , # 9 p. 797 - 801
sodium perchlorate in acetonitrile
in electrochemical cell: Pt anode and cathode; Title compound not separated from byproducts;
参考文献
Kargin, Yu. M.; Nikitin, E. V.; Parakin, O. V.; Romanov, G. V.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1980 , vol. 8, p. 55 - 58
