1,6-二氧螺环[4.4]-壬烷合成路线 （共 33 条）
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
1: With sodium tetrahydroborate; zirconium tetrachloride in tetrahydrofuran T=0 - 20°C; 4 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water Cooling with ice;
参考文献
Mistry, Shailesh N.; Baker, Jillian G.; Fischer, Peter M.; Hill, Stephen J.; Gardiner, Sheila M.; Kellam, Barrie
Journal of Medicinal Chemistry, 2013 , vol. 56, # 10 p. 3852 - 3865
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether T=30°C; 12 h; Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Shaozu, Wu; Tianhui, Ren; Yulan, Zhang
Bulletin des Societes Chimiques Belges, 1991 , vol. 100, # 5 p. 357 - 358
反应条件
diethyl aluminium hydride in hexane; kerosene 30 h; Heating;
参考文献
Volkov; Kravets; Zlot-skii; Rakhmankulov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 7 pt 1 p. 1419 - 1423
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
反应条件
hydrogenchloride T=150°C; 2 h;
参考文献
Musavirov, R. S.; Mullakhmetova, Z. F.; Nedogrei, E. P.; Kantor, E. A.; Rakhmankulov, D. L.; Paushkin, Ya. M.
Doklady Chemistry, 1985 , vol. 284, p. 319 - 321
Dokl. Akad. Nauk SSSR Ser. Khim., 1985 , vol. 284, # 5 p. 1151 - 1154
反应条件
formaldehyd; silica gel; iron(III) chloride T=20°C; 0.0833333 h;
参考文献
Fadel, Antoine; Yefsah, Ramdane; Salauen, Jacques
Synthesis, 1987 , # 1 p. 37 - 40
反应条件
iodo trichloro silane
参考文献
Tetrahedron Letters, , vol. 33, # 12 p. 1657 - 1660
反应条件
Heating; Thermodynamic dataKinetics; PressureConcentrationTimeTemperature;
参考文献
Rosas, Felix; Lezama, Jesus; Mora, Jose R.; Maldonado, Alexis; Chuchani, Gabriel; Cordova, Tania
Journal of Physical Chemistry A: Molecules, Spectroscopy, Kinetics, Environment, and General Theory, 2012 , vol. 116, # 37 p. 9228 - 9237,10
反应条件
Product distribution;
参考文献
Bauduin, G.; Bondon, D.; Pietrasanta, Y.; Pucci, B.
Tetrahedron, 1980 , vol. 36, # 2 p. 245 - 254
