3,5-双(叔丁基)苯甲醛合成路线 （共 43 条）
反应条件
1.1: aluminum trichloride / 24 h 2.1: N-bromosuccinimide; benzoyl peroxide / CCl4 / 3 h / Heating 3.1: hexamethylenetetraamine / methanol; H2O / 4 h / Heating 3.2: 79 g / aq. HCl / methanol / 0.5 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 58, # 12 p. 2405 - 2413
反应条件
1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 78, p. 570,582
反应条件
(i) N-chloro-succinimide, (ii) aq. Na2CO3; Multistep reaction;
参考文献
Synthetic Communications, , vol. 6, p. 575 - 581
反应条件
gold supported on titanium dioxide; oxygen T=20°C; P=760.051 Torr;
参考文献
Laursen, Anders B.; Hojholt, Karen T.; Lundegaard, Lars F.; Simonsen, Soren B.; Helveg, Stig; Schueth, Ferdi; Paul, Michael; Grunwaldt, Jan-Dierk; Kegns, Soren; Christensen, Claus H.; Egeblad, Kresten
Angewandte Chemie - International Edition, 2010 , vol. 49, # 20 p. 3504 - 3507
反应条件
bis(1,5-cyclooctadiene)nickel (0); SlPr in toluene
T=40°C; Tishchenko reaction; 4 h; Inert atmosphere;
参考文献
Hoshimoto, Yoichi; Ohashi, Masato; Ogoshi, Sensuke
Journal of the American Chemical Society, 2011 , vol. 133, # 13 p. 4668 - 4671
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
T=20°C; 1 h; Inert atmosphere;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
1 h;
参考文献
Ambre, Ram; Yu, Chien-Yi; Mane, Sandeep B.; Yao, Ching-Fa; Hung, Chen-Hsiung
Tetrahedron, 2011 , vol. 67, # 25 p. 4680 - 4688
反应条件
1: With trifluoroacetic acid in dichloromethane
T=20°C; 3 h; DarknessInert atmosphere;
2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
T=20°C; 1 h;
3: With triethylamine in dichloromethane
参考文献
Di Carlo, Gabriele; Orbelli Biroli, Alessio; Pizzotti, Maddalena; Tessore, Francesca; Trifiletti, Vanira; Ruffo, Riccardo; Abbotto, Alessandro; Amat, Anna; De Angelis, Filippo; Mussini, Patrizia R.
Chemistry - A European Journal, 2013 , vol. 19, # 32 p. 10723 - 10740
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane
2 h;
2: With chloranil in dichloromethane
1 h; Heating; Further stages.;
参考文献
Richeter, Sebastien; Jeandon, Christophe; Gisselbrecht, Jean-Paul; Ruppert, Romain; Callot, Henry J.
Journal of the American Chemical Society, 2002 , vol. 124, # 21 p. 6168 - 6179
反应条件
1: With boron trifluoride diethyl etherate in chloroform
T=20°C; Inert atmosphereDarkness;
2: With chloranil in chloroform
T=20°C; 6 h; DarknessInert atmosphere;
参考文献
Tamiaki, Hitoshi; Kozawa, Takaaki; Kitamoto, Rika; Kunieda, Michio
Journal of Porphyrins and Phthalocyanines, 2010 , vol. 14, # 5 p. 375 - 388
反应条件
boron trifluoride diethyl etherate in dichloromethane
1 h; Heating;
参考文献
Borovkov, Victor V.; Anikin, Michael; Wasa, Kiyotaka; Sakata, Yoshiteru
Photochemistry and Photobiology, 1996 , vol. 63, # 4 p. 477 - 482
