1,4-二硫杂螺[4.5]癸烷合成路线 （共 34 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; 1-phenyl-propan-1-one in N,N-dimethyl-formamide T=20°C; 0.75 h;
参考文献
Bandgar, Babasaheb P.; Joshi, Neeta S.; Bettigeri, Sampada V.
Monatshefte fur Chemie, 2007 , vol. 138, # 1 p. 67 - 71
反应条件
thionyl chloride; silica gel in toluene 24 h; Heating;
参考文献
Kamitori, Yasuhiro; Hojo, Masaru; Masuda, Ryoichi; Kimura, Tadashi; Yoshida, Tatsushi
Journal of Organic Chemistry, 1986 , vol. 51, # 9 p. 1427 - 1431
反应条件
di-n-butylbis(trifluoromethanesulfonyloxy)stannane in 1,2-dichloro-ethane T=35°C; 10 h;
参考文献
Sato, Tsuneo; Otera, Junzo; Nozaki, Hitosi
Journal of Organic Chemistry, 1993 , vol. 58, # 18 p. 4971 - 4978
反应条件
tetra-n-butylammonium tribromide in tetrahydrofuran T=20°C; 0.08 h;
参考文献
Naik, Sarala; Gopinath, Rangam; Goswami, Mousumi; Patel, Bhisma K.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 11 p. 1670 - 1677
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C; 4 h;
参考文献
Martel, Arnaud; Chewchanwuttiwong, Sopa; Dujardin, Gilles; Brown, Eric
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1491 - 1494
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C; 4 h;
参考文献
Martel, Arnaud; Chewchanwuttiwong, Sopa; Dujardin, Gilles; Brown, Eric
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1491 - 1494
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=-78°C; 4 h;
参考文献
Martel, Arnaud; Chewchanwuttiwong, Sopa; Dujardin, Gilles; Brown, Eric
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1491 - 1494
反应条件
acetyl chloride in methanol 8 h; Heating;
参考文献
Yu, Haifeng; Liu, Qun; Yin, Yanbing; Fang, Qunxin; Zhang, Jingping; Dong, Dewen
Synlett, 2004 , # 6 p. 999 - 1002
反应条件
sodium lauryl sulfate; trichloroacetic acid in water T=70°C; 7 h; chemoselective reaction;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad Mehdi; Tajik, Maryam; Soheilizad, Mehdi
Journal of Sulfur Chemistry, 2011 , vol. 32, # 5 p. 397 - 403
反应条件
mercury dichloride in dichloromethane 24 h; Heating;
参考文献
Jo, Shigeo; Tanimoto, Shigeo; Oida, Tatsuo; Okano, Masaya
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 5 p. 1434 - 1436
