4,4’-二甲氧基二苯基氧化硫合成路线 (共 22 条)
反应条件
in acetic acid T=120 - 125°C; Product distribution;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1957 - 1960
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 30, p. 385
反应条件
thionyl chloride; triphenylphosphine in tetrahydrofuran T=20°C; 4 h; Inert atmosphere;
参考文献
Jang, Yujin; Kim, Kyoung Tae; Jeon, Heung Bae
Journal of Organic Chemistry, 2013 , vol. 78, # 12 p. 6328 - 6331
反应条件
1-phenyl-2,2,2-trifluorodiazoethane; oxygen; 5,15,10,20-tetraphenylporphyrin in dichloromethane; acetonitrile T=20°C; 0.5 h; Irradiation;
参考文献
Ishiguro, Katsuya; Hirano, Yukimichi; Sawaki, Yasuhiko
Tetrahedron Letters, 1987 , vol. 28, # 49 p. 6201 - 6204
反应条件
1: AlCl3 / 125 - 130 °C 2: Erwaermen auf dem Dampfbad 3: CrO3; water; acetic acid 4: aqueous HCl 5: ammonia; diammine zinc-chloride / 200 °C View Scheme
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1947 , vol. 15, p. 129,132
反应条件
1: AlCl3 / 125 - 130 °C 2: Erwaermen auf dem Dampfbad 3: CrO3; water; acetic acid 4: aqueous HCl View Scheme
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1947 , vol. 15, p. 129,132
反应条件
dihydrogen peroxide in acetic acid 0.333333 h; Heating;
参考文献
Bell, Kevin H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1957 - 1960
反应条件
1-phenyl-2,2,2-trifluorodiazoethane; oxygen; 5,15,10,20-tetraphenylporphyrin in dichloromethane; acetonitrile T=20°C; 0.5 h; Irradiation;
参考文献
Ishiguro, Katsuya; Hirano, Yukimichi; Sawaki, Yasuhiko
Tetrahedron Letters, 1987 , vol. 28, # 49 p. 6201 - 6204
参考文献
Smiles; le Rossignol
Journal of the Chemical Society, 1908 , vol. 93, p. 756
Journal of the Chemical Society, 1906 , vol. 89, p. 697
反应条件
aluminium trichloride T=125 - 130°C;
参考文献
Sah
Journal of the Chinese Chemical Society (Peking), 1947 , vol. 15, p. 129,132