反应条件
in tetrahydrofuran
mixt. refluxed for 5h, then hydrolysis of the excess Grignard reagent with satd. aq. NH4Cl; sepn. of the organic layer, drying over MgSO4, filtration, evapn., dissolution in petroleum ether, sepn. on a column containing Kieselgel, twice recrystn. (petroleum ether); elem. anal.;
参考文献
Carson, A. S.; Jamea, E. H.; Laye, P. G.; Spencer, J. A.
Journal of Chemical Thermodynamics, 1988 , vol. 20, # 10 p. 1223 - 1230
