反应条件
KH in dimethyl-ether byproducts: KHBCl3, H2; Me2O and B4H10 condensing onto KH at -196°C under N2, warming slowly to -45°C to remove all the volatiles, BCl3 condensing on theresidue at -196°C, stirring for 2.5-3 h at - 35°C coolingto -196°C, fractionating; identified by IR and NMR spectra;
参考文献
Inorganic Chemistry, , vol. 21, p. 1952 - 1957
