1,3,4,6-四-氧-乙酰-Β-D-吡啶甘露糖合成路线 （共 20 条）
反应条件
hydrogenchloride in water
参考文献
Acta Crystallographica Section C: Crystal Structure Communications, , vol. 68, # 9 p. o338-o340
反应条件
diethyl ether; silver(I) acetate
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 247,249; engl. Ausg. S. 303, 304
反应条件
1: ammonia; diethyl ether 2: silver acetate; diethyl ether View Scheme
参考文献
Zhurnal Obshchei Khimii, , vol. 22, p. 247,249; engl. Ausg. S. 303, 304
反应条件
Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1329 - 1331
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1638 - 1641
参考文献
Journal of the American Chemical Society, , vol. 80, p. 3372,3378
Journal of the American Chemical Society, , vol. 81, p. 5171,5172, 5176
反应条件
pyridine in dichloromethane -15 deg C to 5 deg C;
参考文献
Pozsgay; Glaudemans; Robbins; Schneerson
Tetrahedron, 1992 , vol. 48, # 47 p. 10249 - 10264
反应条件
pyridine; trifluoromethanesulfonic acid anhydride in dichloromethane
参考文献
The Trustees of Princeton University
Patent: US6040433 A1, 2000 ;
反应条件
1: 93 percent / pyridine / CH2Cl2 / -20 - -10 °C 2: 1) sodium azide, 2) pyridine / 1) 2-methoxyethanol, 100 deg C, overnight, 2) 2 h View Scheme
参考文献
Pavliak, Viliam; Kovac, Pavol
Carbohydrate Research, 1991 , vol. 210, p. 333 - 337
反应条件
1: 50 percent / pyridine / 2 h / -20 - 0 °C
2: 50 percent / aq. HCl / 0.5 h / Heating
3: 500 mg / tetraethylammonium fluoride dihydrate / acetonitrile; tetrahydrofuran / 20 °C
View Scheme
参考文献
De Groot, Tjibbe; Bormans, Guy; Busson, Roger; Mortelmans, Luc; Verbruggen, Alfons
Journal of Labelled Compounds and Radiopharmaceuticals, 1999 , vol. 42, # 2 p. 147 - 157
反应条件
1: pyridine / CH2Cl2
2: NaN3 / dimethylformamide
View Scheme
参考文献
Pavliak, Viliam; Kovac, Pavol
Carbohydrate Research, 1991 , vol. 210, p. 333 - 337
