in tetrachloromethane byproducts: tert-butyl phenyl ether, tert-C4H9OH; sealed evacuated H-shaped ampuls; react. of Ph3BiCl2 and Li-compd. in CCl4 at 20°C (60 h); transcondensation of lig. products with cooling (liq. N2) into a limb of the ampul, hydrolyzation of solid residue by aq. THF, codensation of alcohol into a trap (liq. N2), treatement of solid residue (hexane, water); detn. of lig. products by GLC anal.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 54, p. 87 - 89
Zhurnal Obshchei Khimii, , vol. 54, p. 100 - 103
in tetrachloromethane T=20°C; 60 h; in the end the hydronysis by 15percent aqueous THF, other solvent, other time, other temperature; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 1 p. 100 - 103,87 - 89
