3,4,5-三甲氧基苯甲酸甲酯合成路线 (共 184 条)
反应条件
sodium hydroxide; potassium carbonate; dimethyl sulfate 1.) aq. EtOH, reflux, 10 h; 2.) acetone, rt., 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3039 - 3055
反应条件
sodium methylate 1.) methanol, RT, 16 h, 2.) ether, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 8 p. 1765 - 1772
反应条件
sodium hydroxide 1.) acetone, 80 deg C, 30 min; 2.) ether, 1 h; Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 369 - 376
反应条件
sodium hydroxide 1.) MeOH, reflux, 2.5 h, 2.) ether, 30 min; Yield given. Multistep reaction;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1067 - 1074
反应条件
hydrogenchloride; sodium hydroxide 1.) reflux, 40 min; 3.) ether, 10 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 1 p. 217 - 220
反应条件
in methanol 85 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 163 - 172
反应条件
sodium methylate; potassium carbonate 1.) acetone, a.) RT, overnight, b.) reflux, 7 h, 2.) MeOH, RT, overnight; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 2 p. 338 - 342
反应条件
sodium hydroxide; potassium carbonate 1.) aq. EtOH, reflux, 10 h; 2.) acetone, rt., 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 31, # 9 p. 3039 - 3055
参考文献
Bulletin of the Korean Chemical Society, , vol. 35, # 4 p. 987 - 988
参考文献
Chemische Berichte, , vol. 41, p. 1772