N-苯基-2-呋喃羧酰胺合成路线 (共 28 条)
反应条件
1: P2S5 / pyridine 2: baker's yeast 3: 74 percent / POCl3 / 2 h / 100 °C View Scheme
参考文献
Paizs, Csaba; Tosa, Monica; Majdik, Cornelia; Taehtinen, Petri; Irimie, Florin Dan; Kanerva, Liisa T.
Tetrahedron Asymmetry, 2003 , vol. 14, # 5 p. 619 - 627
反应条件
oxygen; lithium hydroxide hydrate in water
T=50°C; 12 h;
参考文献
Wang, Ye; Zhu, Dapeng; Tang, Lin; Wang, Sujing; Wang, Zhiyong
Angewandte Chemie - International Edition, 2011 , vol. 50, # 38 p. 8917 - 8921
反应条件
triethylamine in dichloromethane
T=20°C; 3 h; regioselective reaction;
参考文献
Laidaoui, Nouria; Roger, Julien; Miloudi, Abdellah; El Abed, Douniazad; Doucet, Henri
European Journal of Organic Chemistry, 2011 , # 23 p. 4373 - 4385
反应条件
copper(l) iodide; acetaldehyde oxime; potassium carbonate; N-methyl-2-(methylamino)ethylamine in toluene
T=120°C; 15 h; Inert atmosphereSchlenk technique;
参考文献
Zhang, Dong-Xue; Xiang, Shi-Kai; Hu, Hao; Tan, Wen; Feng, Chun; Wang, Bi-Qin; Zhao, Ke-Qing; Hu, Ping; Yang, Hua
Tetrahedron, 2013 , vol. 69, # 47 p. 10022 - 10029
反应条件
1: furan-2-carboxylic acid With iodine; triethylamine; phosphorous acid trimethyl ester in ethyl acetate
0.166667 h; Cooling with iceInert atmosphere;
2: aniline in ethyl acetate
T=20°C; 3 h; Inert atmosphereCooling with ice;
参考文献
Luo, Qun-Li; Lv, Lina; Li, Yu; Tan, Jian-Ping; Nan, Wenhui; Hui, Qun
European Journal of Organic Chemistry, 2011 , # 34 p. 6916 - 6922
反应条件
triethylamine; 3,4,5-tmtz iodide in N,N-dimethyl-formamide
T=75°C; 20 h; Heating;
参考文献
Castells, J.; Pujol, F.; Llitjos, H.; Moreno-Manas, M.
Tetrahedron, 1982 , vol. 38, # 3 p. 337 - 346
反应条件
CuSO4‵5H2O; potassium carbonate; N-methyl-2-(methylamino)ethylamine in o-xylene
T=130°C; 12 h; regioselective reaction;
参考文献
Panda, Niranjan; Mothkuri, Raghavender; Nayak, Dinesh Kumar
European Journal of Organic Chemistry, 2014 , vol. 2014, # 8 p. 1602 - 1605
反应条件
samarium diiodide in tetrahydrofuran
T=65°C; 0.166667 h;
参考文献
Li, Xue; Zhang, Yongmin
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2006 , vol. 45, # 6 p. 1576 - 1578
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in N,N-dimethyl-formamide
T=60°C; 0.05 h; Microwave irradiation;
参考文献
Kumar, Katari Naresh; Sreeramamurthy, Kintali; Palle, Sadananda; Mukkanti, Khagga; Das, Parthasarathi
Tetrahedron Letters, 2010 , vol. 51, # 6 p. 899 - 902
反应条件
magnesium trifluoromethane sulfonate in toluene
T=110°C; 16 h;
参考文献
Gertzmann; Guertler
Tetrahedron Letters, 2005 , vol. 46, # 39 p. 6659 - 6662