N-苯基-2-呋喃羧酰胺合成路线 （共 28 条）
反应条件
tetrabutyl ammonium fluoride; copper diacetate in N,N-dimethyl-formamide
T=20°C;
参考文献
Lam, Patrick Y.S.; Deudon, Sophie; Hauptman, Elisabeth; Clark, Charles G.
Tetrahedron Letters, 2001 , vol. 42, # 13 p. 2427 - 2429
反应条件
PEG-400; potassium carbonate in acetonitrile
Substitution; 0.25 h; Heating;
参考文献
Wei, Tai-Bao; Zhang, You-Ming
Synthetic Communications, 1999 , vol. 29, # 17 p. 2943 - 2947
反应条件
nitrobenzene; triethylamine; 3,4,5-tmtz iodide
T=80°C; 48 h; Heating;
参考文献
Castells, J.; Pujol, F.; Llitjos, H.; Moreno-Manas, M.
Tetrahedron, 1982 , vol. 38, # 3 p. 337 - 346
反应条件
nitrobenzene; triethylamine; 3,4,5-tmtz iodide
T=80°C; 216 h; Heating;
参考文献
Castells, J.; Pujol, F.; Llitjos, H.; Moreno-Manas, M.
Tetrahedron, 1982 , vol. 38, # 3 p. 337 - 346
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide
T=120°C; Heck reaction; 36 h; Inert atmosphere;
参考文献
Kee, Chin Hui; Ariffin, Azhar; Awang, Khalijah; Takeya, Koichi; Morita, Hiroshi; Hussain, Salmaan Inayat; Chan, Kok Meng; Wood, Pauline J.; Threadgill, Michael D.; Lim, Chuan Gee; Ng, Seikweng; Weber, Jean Frederic F.; Thomas, Noel F.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 24 p. 5646 - 5660
反应条件
diethyl ether
anschliessend Hydrolyse;
参考文献
Gilman et al.
Journal of the American Chemical Society, 1932 , vol. 54, p. 733,735
反应条件
1: SOCl2 / 0.5 h / Heating
2: triethylamine / CH2Cl2 / 1 h / Heating
View Scheme
参考文献
Lee, Chang Kiu; Yu, Ji Sook; Ji, Young Ran
Journal of Heterocyclic Chemistry, 2002 , vol. 39, # 6 p. 1219 - 1227
反应条件
in acetonitrile
T=60°C; 2 h; Yield given;
参考文献
Kitagawa, Tokujiro; Kuroda, Hiroko; Sasaki, Hideaki; Kawasaki, Koichi
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 10 p. 4294 - 4301
反应条件
1: sodium hydroxide; oxygen / water / 12 h / 40 °C
2: sodium hydroxide; oxygen / water / 18 h / 40 °C / |Green chemistry
View Scheme
参考文献
Zhang, Leilei; Wang, Wentao; Wang, Aiqin; Cui, Yitao; Yang, Xiaofeng; Huang, Yanqiang; Liu, Xiaoyan; Liu, Wengang; Son, Jin-Young; Oji, Hiroshi; Zhang, Tao
Green Chemistry, 2013 , vol. 15, # 10 p. 2680 - 2684
反应条件
aluminum oxide
T=310°C;
参考文献
Jur'ew; Wendelschtein
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 259; engl. Ausg. S. 281
