反应条件
1: 1,1-dimethylethylmagnesium chloride With bis(acetylacetonate)nickel(II); 1-(2-carboxyethyl)-3-mesityl-1H-imidazol-3-ium chloride; lithium tert-butylate in tetrahydrofuran; diethyl ether T=0°C; 0.166667 h; Inert atmosphere; 2: 9-fluorenyl bromide in tetrahydrofuran; diethyl ether T=0 - 20°C; Kumada-Corriu-Tamao type reaction; Inert atmosphere;
参考文献
Lohre, Claudia; Droege, Thomas; Wang, Congyang; Glorius, Frank
Chemistry - A European Journal, 2011 , vol. 17, # 22 p. 6052 - 6055
