1: tert-butyl alcohol With n-butyllithium in hexane T=20 - 30°C; 0.5 h; 2: 4-nitro-benzoyl chloride in diethyl ether; hexane T=20 - 30°C; 3 h;
参考文献
THE UNITED STATES GOVERNMENT as represented by THE DEPARTMENT OF HEALTH AND HUMAN SERVICES
Patent: EP1367046 A1, 2003 ;
Location in patent: Page 24 ;
EP 1367046 A1
