1-(苯基乙炔基)-1-环己醇合成路线 （共 34 条）
反应条件
(i) LiNEt2, THF, (ii) /BRN= 385735/; Multistep reaction;
参考文献
Organometallics in Chemical Synthesis, , vol. 1, p. 393 - 414
参考文献
Schering A.G.
Patent: US2816910 , 1953 ;
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Schering A.G.
Patent: DE1007764 , 1952 ;
反应条件
silver(I) acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene in 1,4-dioxane T=110°C; 15 h; Autoclave;
参考文献
Qi, Chaorong; Huang, Liangbin; Jiang, Huanfeng
Synthesis, 2010 , # 9 art. no. F23909SS, p. 1433 - 1440
反应条件
water in dimethyl sulfoxide T=80°C; 1 h;
参考文献
Schmidt, Elena Yu; Zorina, Nadezhda V.; Skitaltseva, Elena V.; Ushakov, Igor A.; Mikhaleva, Albina I.; Trofimov, Boris A.
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3772 - 3775
反应条件
formic acid 3 h; Heating;
参考文献
Marson; Walker; Pickering; Harper; Wrigglesworth; Edge
Tetrahedron, 1993 , vol. 49, # 45 p. 10317 - 10338
反应条件
copper(l) iodide; diisopropylamine; bis-triphenylphosphine-palladium(II) chloride
T=80°C;
参考文献
Csekei, Marton; Novak, Zoltan; Kotschy, Andras
Tetrahedron, 2008 , vol. 64, # 6 p. 975 - 982
反应条件
methanesulfonyl chloride; triethylamine in dichloromethane
T=-20°C; stereoselective reaction;
参考文献
Belov, Dmitry S.; Lukyanenko, Evgeny R.; Kurkin, Alexander V.; Yurovskaya, Marina A.
Journal of Organic Chemistry, 2012 , vol. 77, # 22 p. 10125 - 10134
反应条件
copper(l) iodide; lithium carbonate in dichloromethane
T=70°C; Inert atmosphere; regioselective reaction;
参考文献
Xu, Ze-Feng; Cai, Chen-Xin; Liu, Jin-Tao
Organic Letters, 2013 , vol. 15, # 9 p. 2096 - 2099
反应条件
triethylsilane in 1,2-dichloro-ethane
T=50°C; 1.5 h;
参考文献
Egi, Masahiro; Kawai, Takuya; Umemura, Megumi; Akai, Shuji
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 7092 - 7097
反应条件
pentafluorophenyldihydroxyborane in 1,2-dichloro-ethane
16 h; Molecular sieveReflux;
参考文献
McCubbin, J. Adam; Nassar, Costa; Krokhin, Oleg V.
Synthesis, 2011 , # 19 art. no. M61711SS, p. 3152 - 3160
