reagiert analog mit Aethylmagnesiumbromid und Benzylmagnesiumbromid;
参考文献
Gilman; Morris
Journal of the American Chemical Society, 1926 , vol. 48, p. 2403
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Sonn; Schmidt
Chemische Berichte, 1924 , vol. 57, p. 1355
Zeifman,Yu.V. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1979 , vol. 28, p. 366 - 368
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1979 , vol. 28, p. 396 - 398
triphenylphosphine in tetrahydrofuran under N2, mixt. of Fe-complex, C6H4NSO and PPh3 (molar ratio 1:1:2) in THF were stirred for 1-4 h at room temp.; solvent removed at reduced pressure, chromd. on alumina column (CH2Cl2), recrystd. from CH2Cl2-hexane; elem. anal.;
参考文献
Ashton, Henry C.; Manning, A. R.
Inorganic Chemistry, 1983 , vol. 22, p. 1440 - 1445
in Petroleum ether decompn. of thioaniline dissolved in dild. petroleum (b.p. 200-250°C) on introduction of dry HCl (shaking) at -10°C;; filtration (anilinium chloride); fractionation;;
参考文献
Bulletin de la Societe Chimique de France, , vol. 6, p. 579 - 580
