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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
22493-94-3
合成路线
（共 20 条）
75-97-8
频哪酮
→
反应条件
22493-94-3
反应条件
potassium hydroxide in ethanol; water T=95°C;
参考文献
Parekh, Vimal; Ramsden, James A.; Wills, Martin
Tetrahedron Asymmetry, 2010 , vol. 21, # 11-12 p. 1549 - 1556
91-22-5
喹啉
→
反应条件
22493-94-3
反应条件
1: in tetrahydrofuran T=20°C; 3 h; 2: With boric acid trimethyl ester 1 h; 3: With water 0.5 h; regioselective reaction;
参考文献
Seo, Hye Ji; Yoon, Soo Jung; Jang, So Hyun; Namgoong, Sung Keon
Tetrahedron Letters, 2011 , vol. 52, # 29 p. 3747 - 3750
91-22-5
喹啉
→
反应条件
22493-94-3
反应条件
1: acetonitrile / 0.5 h / 0 °C 2: NaI / acetonitrile / 0.17 h / 50 °C 3: 63 percent / Et3N / CH2Cl2 / 2 h / 20 °C 4: 25 percent / TMEDA / tetrahydrofuran; hexane / 0.5 h / -70 °C View Scheme
参考文献
Haase, Mirko; Guenther, Wolfgang; Goerls, Helmar; Anders, Ernst
Synthesis, 1999 , # 12 p. 2071 - 2081
917-92-0
3,3-二甲基-1-丁炔
+
529-23-7
2-氨基苯甲醛
→
反应条件
22493-94-3
反应条件
C46H44Ag2Fe2N6O2; aniline in 1,2-dichloro-ethane 8 h; Inert atmosphereSchlenk techniqueSealed tubeHeating; regioselective reaction;
参考文献
Sarbajna, Abir; Sadhukhan, Nabanita; Saha, Sayantani; Bera, Jitendra K
Indian Journal of Chemistry - Section A Inorganic, Physical, Theoretical and Analytical Chemistry, 2013 , vol. 52, # 8-9 p. 1072 - 1077
1613-37-2
喹啉-N-氧化物
+
38442-51-2
→
反应条件
22493-94-3
+
78324-96-6
反应条件
sodium thiosulfate; potassium iodide 1.) DMSO, 35-40 deg C, 4 h, irradiation; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Russell, Glen A.; Wang, Lijuan; Yao, Ching-Fa
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5390 - 5395
38442-51-2
→
反应条件
22493-94-3
+
78324-96-6
反应条件
toluene-4-sulfonic acid; potassium iodide 1.) DMSO, 35-40 deg C, 10 min, irradiation, 2.) 85 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russell, Glen A.; Wang, Lijuan; Yao, Ching-Fa
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5390 - 5395
38442-51-2
→
反应条件
22493-94-3
反应条件
sodium thiosulfate; potassium iodide 1.) DMSO, 35-40 deg C, 10 min, irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russell, Glen A.; Wang, Lijuan; Yao, Ching-Fa
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5390 - 5395
91-22-5
喹啉
+
75-98-9
特戊酸
→
反应条件
22493-94-3
+
115-11-7
异丁烯
+
75-65-0
叔丁醇
反应条件
dipotassium peroxodisulfate; sulfuric acid; copper diacetate; silver nitrate in water T=57°C; 3 h; (NH4)2S2O8 for K2S2O8; Rate constantProduct distribution;
参考文献
Citterio, Attilio; Minisci, Francesco; Franchi, Valeria
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4752 - 4757
38442-51-2
→
反应条件
22493-94-3
+
78324-96-6
反应条件
sodium thiosulfate; potassium iodide 1.) DMSO, 35-40 deg C, 10 min, irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russell, Glen A.; Wang, Lijuan; Yao, Ching-Fa
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5390 - 5395
38442-51-2
→
反应条件
22493-94-3
反应条件
sodium methylate; potassium iodide 1.) DMSO, 35-40 deg C, 10 min, irradiation, 2.) 85 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Russell, Glen A.; Wang, Lijuan; Yao, Ching-Fa
Journal of Organic Chemistry, 1995 , vol. 60, # 17 p. 5390 - 5395
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