3,3',5,5'-四叔丁基-4,4'-联苯醌合成路线 (共 172 条)
反应条件
lead dioxide in water T=25°C; 0.0833333 h; Further byproducts.;
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867
反应条件
1: With 5 palladium on charcoal; potassium acetate in water T=100°C; 0.333333 h; 2: With oxygen in water 8 h;
参考文献
Organic Process Research and Development, , vol. 9, # 1 p. 62 - 69
反应条件
1: 4-bromo-2,6-di-tert-butylphenol With sodium hydride in 1-methyl-pyrrolidin-2-one; mineral oil T=20°C; 0.5 h; Inert atmosphereCooling with ice; 2: N,N-dimethylthiocarbamoyl chloride in 1-methyl-pyrrolidin-2-one; mineral oil T=80°C; 4 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 79, # 5 p. 2082 - 2093
反应条件
N-(2',4'-dichloro-6'-oxo-2',4'-cyclohexadien-1'-ylidene)-4-nitrobenzamide in dichloromethane 16 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 13 p. 4039 - 4043
反应条件
3-methoxy-phenol; copper; potassium carbonate in pyridine T=180°C; 4 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 493 - 497
反应条件
trifluoroacetic acid in benzene varying time-interval before addition of reag.; Product distribution;
参考文献
Tetrahedron, , vol. 51, # 25 p. 6901 - 6910
反应条件
potassium tert-butylate; oxygen in tert-butyl alcohol 1.5 h;
参考文献
Liebigs Annales, , # 7 p. 1183 - 1186
反应条件
lead dioxide; trifluoroacetic acid T=25°C;
参考文献
Synthesis, , # 8 p. 1145 - 1148
反应条件
triethylamine in n-heptane 72 h; Ambient temperature; Mechanism;
参考文献
Journal of Organic Chemistry, , vol. 49, # 26 p. 5260 - 5262
反应条件
manganese triacetate in acetic acid T=100°C; 0.166667 h; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 2 p. 620 - 622