253185-03-4合成路线 (共 388 条)
参考文献
Stock; Brown
Journal of the American Chemical Society, 1959 , vol. 81, p. 5615,5617, 5620
参考文献
de la Mare; Harvey
Journal of the Chemical Society, 1957 , p. 131,134
反应条件
T=200 - 350°C; in der Dampfphase;
参考文献
Duffin et al.
Journal of the Chemical Society, 1959 , p. 2734,2740
参考文献
Curtin; Leskowitz
Journal of the American Chemical Society, 1951 , vol. 73, p. 2630,2632
反应条件
AlCl3, aluminium chloride in dichloromethane T=10°C; 0.5 h; Inert atmosphere;
参考文献
Tiruveedhula, V.V.N. Phani Babu; Witzigmann, Christopher M.; Verma, Ranjit; Kabir, M. Shahjahan; Rott, Marc; Schwan, William R.; Medina-Bielski, Sara; Lane, Michelle; Close, William; Polanowski, Rebecca L.; Sherman, David; Monte, Aaron; Deschamps, Jeffrey R.; Cook, James M.
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 24 p. 7830 - 7840
反应条件
1: 53 percent / AlCl3, urea / 3 h / 0 - 5 °C 2: 34 percent / AcOH / 2 h / Heating View Scheme
参考文献
Freyer, Wolfgang
Journal fuer Praktische Chemie/Chemiker-Zeitung, 1994 , vol. 336, # 8 p. 690 - 692
参考文献
Journal of the American Chemical Society, , vol. 81, p. 5611,5612
参考文献
Journal of the American Chemical Society, , vol. 76, p. 1906
反应条件
carbon disulfide; aluminium trichloride
参考文献
Kim, Soo-Kang; Park, Young-Il; Park, Jong-Wook; Kim, Kyoung-Soo; Choi, Cheol-Kyu; Lee, Sang-Do
Molecular Crystals and Liquid Crystals, 2007 , vol. 462, # 1 p. 209 - 216
反应条件
1: 84 percent / Br2, Fe / CCl4 / 1 h / 0 °C 2: 65.4 percent / KOH / Cu / 1.) 150 deg C, 1 h, 2.) 180-200 deg C, 4 h 3: 38.1 percent / TiCl4 / CH2Cl2 / 5 h / 0 °C 4: 81.1 percent / AlH2Cl / diethyl ether / 24 h / Heating 5: 80 percent / Nafion-H, toluene / 24 h / Heating View Scheme
参考文献
Yamato, Takehiko; Komine, Masayasu; Nagano, Yoshiaki
Organic Preparations and Procedures International, 1997 , vol. 29, # 3 p. 300 - 303