2,2-二甲基-3-氧代-3-苯基丙酸乙酯合成路线 (共 31 条)
反应条件
1,1,1,2,2,2-hexabutyl-distannane in cyclohexane 36 h; Irradiation;
参考文献
Best, Wayne M.; Cook, Anthony P. F.; Russell, James J.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1139 - 1144
反应条件
1: 1.) NaH, 60percent in oil / 1.) DMSO, until homogeneous; 2.) DMSO, overnight 2: 28 percent Chromat. / (Bu3Sn)2 / cyclohexane / 36 h / Irradiation View Scheme
参考文献
Best, Wayne M.; Cook, Anthony P. F.; Russell, James J.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1139 - 1144
反应条件
mercury dichloride; zinc in benzene Heating;
参考文献
Heng Suen,Y.; Kagan,H.B.
Bulletin de la Societe Chimique de France, 1965 , p. 1460 - 1463
反应条件
in dichloromethane Ambient temperature;
参考文献
Reddy, Chaganti P.; Tanimoto, Shigeo
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 411 - 414
参考文献
Hope; Perkin
Journal of the Chemical Society, 1909 , vol. 95, p. 2046
参考文献
Blaise; Courtot
Bulletin de la Societe Chimique de France, 1906 , vol. <3> 35, p. 591,597
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1905 , vol. 141, p. 725
参考文献
Lapin,H.; Horeau,A.
Gazzetta Chimica Italiana, 1963 , vol. 93, p. 451 - 454
反应条件
lithium hydroxide 1.) THF, 55 deg C, 15 min, 2.) THF, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Antonioletti, Roberto; Bonadies, Francesco; Orelli, Liliana Raquel; Scettri, Arrigo
Gazzetta Chimica Italiana, 1992 , vol. 122, # 5-7 p. 237 - 238
参考文献
Bloom; Hauser
Journal of the American Chemical Society, 1944 , vol. 66, p. 153
参考文献
Hudson; Dick; Hauser
Journal of the American Chemical Society, 1938 , vol. 60, p. 1961
Full Text Show Details
Scheibler; Stein
Journal fuer Praktische Chemie (Leipzig), 1934 , vol. <2> 139, p. 105,107