(S)-(+)-2-戊醇合成路线 （共 77 条）
反应条件
0.5 h; Resolution of racemate; optical yield given as percent ee;
参考文献
Akazome, Motohiro; Toma, Shusaku; Horiguchi, Tatsunori; Megumi, Ken; Matsumoto, Shoji
Tetrahedron, 2011 , vol. 67, # 16 p. 2844 - 2848
参考文献
Goergens, Ulrich; Schneider, Manfred P.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 9 p. 1149 - 1152
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B immobilized on acrylic resin catalyst in pentane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B catalyst in n-heptane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B catalyst in n-heptane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
Candida antarctica lipase B catalyst in n-heptane T=20 - 25°C; 24 h; Enzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Strohalm, Hedwig; Dold, Susanne; Pendzialek, Kathrin; Weiher, Monika; Engel, Karl-Heinz
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 10 p. 6328 - 6333
反应条件
sodium hydroxide; (-)-isopinocampheylborane; dihydrogen peroxide 1) THF, -25 deg C, 9 h, 2) 50 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Brown, Herbert C.; Jadhav, Prabhakar K.; Mandal, Arun K.
Journal of Organic Chemistry, 1982 , vol. 47, # 26 p. 5074 - 5083
