N-甲基-N-苯基乌拉坦合成路线 （共 19 条）
反应条件
bisallyl ether; triphenylphosphine in 1,4-dioxane T=18 - 20°C; 5 h;
参考文献
Parfenov, E. A.; Fomin, V. A.
J. Gen. Chem. USSR (Engl. Transl.), 1981 , vol. 51, # 5 p. 1144 - 1153,961 - 968
反应条件
in 1,2-dichloro-benzene
参考文献
Bayer Aktiengesellschaft
Patent: US4439591 A1, 1984 ;
反应条件
copper(l) iodide; oxygen 12 h; Ambient temperature;
参考文献
Chen, Chih-Cheng; Chen, Same-Ting; Chuang, Tsung-Hsun; Fang, Jim-Min
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 16 p. 2217 - 2222
反应条件
1: 91 percent / LDA / tetrahydrofuran / 0.75 h / -40 °C 2: 64 percent / CuI, O2 / 12 h / Ambient temperature View Scheme
参考文献
Chen, Chih-Cheng; Chen, Same-Ting; Chuang, Tsung-Hsun; Fang, Jim-Min
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 16 p. 2217 - 2222
反应条件
diethyl ether; toluene
参考文献
Leister; Tarbell
Journal of Organic Chemistry, 1958 , vol. 23, p. 1152,1155
反应条件
in 1,4-dioxane T=25°C; ΔH(excit.), ΔS(excit.), different temp.; Rate constantThermodynamic data;
参考文献
Schmidt,O.
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, 1907 , vol. 58, p. 517,523
Chemische Berichte, 1903 , vol. 36, p. 2476
反应条件
diethylzinc 1.) benzene, 160 deg C, 50 atm, 5 h; 2.) benzene, 140 deg C, 20 h; other temp.; Product distribution;
参考文献
Yoshida; Ishii; Kawato; Yamashita; Yano; Inoue
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, # 8 p. 2913 - 2916
反应条件
sodium 1.) HMPT, ether, 15 min; 2.) ether, r.t., 30 min; Yield given. Multistep reaction;
参考文献
Dembele, Albert; Deshayes, Henri; Pete, Jean-Pierre
Bulletin de la Societe Chimique de France, 1988 , # 4 p. 671 - 680
参考文献
Diels
Chemische Berichte, 1923 , vol. 56, p. 1936
参考文献
Schmidt,O.
Chemische Berichte, 1903 , vol. 36, p. 2476
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, 1907 , vol. 58, p. 516
