N-(2-氯乙基)苯甲酰胺合成路线 (共 47 条)
反应条件
in diethyl ether; ethanol (thermolysis);
参考文献
Pelz,K. et al.
Collection of Czechoslovak Chemical Communications, 1968 , vol. 33, # 6 p. 1880 - 1894
参考文献
Gabriel; Stelzner
Chemische Berichte, 1895 , vol. 28, p. 2933
反应条件
ammonium hydroxide; hydrazine hydrate 1) CHCl3, 1 h, 20 deg C, 2) MeOH, 45 min, 60 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Neumann, R.; Beger, J.
Journal fuer Praktische Chemie (Leipzig), 1982 , vol. 324, # 6 p. 1026 - 1032
反应条件
bis(tri-n-butyltin)oxide 2.) r.t., 10 min; Yield given. Multistep reaction;
参考文献
Shibata, Ikuya; Nakamura, Kenji; Baba, Akio; Matsuda, Haruo
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 3 p. 853 - 859
反应条件
2: ethanolic sodium ethylate 3: diethyl ether; ethanol; hydrogen chloride / 4 °C View Scheme
参考文献
Goldberg; Kelly
Journal of the Chemical Society, 1948 , p. 1919,1925
反应条件
1: ethanolic sodium ethylate 2: diethyl ether; ethanol; hydrogen chloride / 4 °C View Scheme
参考文献
Goldberg; Kelly
Journal of the Chemical Society, 1948 , p. 1919,1925
参考文献
Gen. Aniline and Film Corp.
Patent: US2288178 , 1939 ;
参考文献
Partridge; Turner
Journal of the Chemical Society, 1949 , p. 1308
参考文献
Wislicenus,W.; Koerber
Chemische Berichte, 1902 , vol. 35, p. 167
反应条件
n-butyllithium; naphthalenyllithium in tetrahydrofuran; hexane 1.) -78 deg C, 8 h, 2.) -78 deg C, 1 h; -78 deg C to r.t., overnight;
参考文献
Journal of Organic Chemistry, , vol. 58, # 22 p. 5976 - 5980