3-溴-3-甲基-2-丁酮合成路线 （共 48 条）
参考文献
Faworski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1361
Chem. Zentralbl., 1913 , vol. 84, # I p. 1007
参考文献
Faworski
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1912 , vol. 44, p. 1361
Chem. Zentralbl., 1913 , vol. 84, # I p. 1007
参考文献
Temnikowa; Oschuewa
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3730; engl. Ausg. S. 3686
反应条件
1: sodium azide / methanol; H2O / 1.5 h / Heating 2: conc. hydrochlorid acid, H2 / 10 percent palladium-charcoal / ethanol 3: 80 percent / ethanol; H2O 4: 72 percent / triethylamine, / ethanol / 16 h / Heating 5: 79 percent / 2M hydrochloric acid / H2O / 0.5 h / Heating 6: 76 percent / sodium dithionite / aq. NaOH / Heating View Scheme
参考文献
Al-Hassan, Saiba S.; Cameron, Robert J.; Curran, Adrian W. C.; Lyall, William J. S.; Nicholson, Sydney H.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1985 , p. 1645 - 1660
参考文献
Aston; Greenburg
Journal of the American Chemical Society, 1940 , vol. 62, p. 2593
反应条件
1: (i) NaOH, EtOH, (ii) /BRN= 1742523/ 2: NH2OH*HCl, Py 3: Na, liq. NH3 4: LiAlH4 / diethyl ether 5: H2O / Raney-Ni View Scheme
参考文献
Stacy,G.W. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 592 - 597
参考文献
Aston; Greenburg
Journal of the American Chemical Society, 1940 , vol. 62, p. 2593
参考文献
Aston; Greenburg
Journal of the American Chemical Society, 1940 , vol. 62, p. 2593
反应条件
(i) KOAc, MeOH, (ii) /BRN= 1742523/; Multistep reaction;
参考文献
Humphlett,W.J.; Lamon,R.W.
Journal of Organic Chemistry, 1964 , vol. 29, p. 2146 - 2148
参考文献
Venus-Danilowa
Zhurnal Obshchei Khimii, 1941 , vol. 11, p. 849
Chem.Abstr., 1942 , p. 4095
