雄甾-3-酮-4-烯-17bata-羧酸甲酯合成路线 （共 22 条）
反应条件
acetone; sodium iodide Erwaermen des Reaktionsprodukts mit Zink-Pulver und Aethanol;
参考文献
Sallmann; Tamm
Helvetica Chimica Acta, 1956 , vol. 39, p. 1340,1360
反应条件
acetone; sodium iodide Erwaermen des Reaktionsprodukts mit Zink-Pulver und Aethanol;
参考文献
Sallmann; Tamm
Helvetica Chimica Acta, 1956 , vol. 39, p. 1340,1360
反应条件
aluminum isopropoxide; toluene
参考文献
Miescher; Wettstein
Helvetica Chimica Acta, 1939 , vol. 22, p. 1262,1265
反应条件
sodium azide 22 h; Ambient temperature;
参考文献
Annen, Klaus; Hofmeister, Helmut; Laurent, Henry; Hoyer, Georg-Alexander
Liebigs Annalen der Chemie, 1989 , p. 991 - 996
参考文献
Sallmann; Tamm
Helvetica Chimica Acta, 1956 , vol. 39, p. 1340,1360
反应条件
Erhitzen des Reaktionsprodukts mit Essigsaeure;
参考文献
Lardon
Helvetica Chimica Acta, 1949 , vol. 32, p. 1517,1528
参考文献
Miescher; Wettstein
Helvetica Chimica Acta, 1939 , vol. 22, p. 1262,1265
反应条件
potassium hydroxide in methanol Hydrolysis; 5 h; Heating;
参考文献
Xia, Peng; Yang, Zheng-Yu; Xia, Yi; Zheng, Yun-Qing; Cosentino, L.Mark; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry, 1999 , vol. 7, # 9 p. 1907 - 1911
反应条件
1: 100 percent / aq. KOH / methanol / 5 h / Heating 2: SOCl2; pyridine / toluene / 3 h / 5 °C 3: 1.50 g / toluene / 0.5 h / 5 °C View Scheme
参考文献
Fei, Xiang-Shu; Tian, Wei-Sheng; Chen, Qing-Yun
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 24 p. 3113 - 3118
反应条件
1: 85 percent / PBr3 / acetic acid / 21 h / Ambient temperature 2: 96 percent / KOH / methanol / 24 h / Heating 3: (COCl)2 / toluene / 4 h / Ambient temperature 4: toluene / 0.5 h / Ambient temperature View Scheme
参考文献
Baine, Neil H.; Owings, Franklin F.; Kline, Donald N.; Resnick, Theodore; Ping, Li-Jen; et al.
Journal of Organic Chemistry, 1994 , vol. 59, # 20 p. 5987 - 5989
