in neat (no solvent)
heating of solid NaCl and liquid N2O4 at 100°C in bomb tube;;
参考文献
Partington, J. R.; Whynes, A. L.
Journal of the Chemical Society, 1949 , p. 3135 - 3141
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
Robbins, R. C.; Cadle, R. D.; Eckhardt, D. L.
J. Meteorol., 1959 , vol. 16, p. 53 - 56
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
in sulfuric acid
passing SO2 into fuming HNO3 at 5°C under formation of NOHSO4; addn. of concd. H2SO4; treatment of soln. with hot air steam under heating; passing dry HCl into soln. at 55°C;;
参考文献
Coleman, G. H.; Gillis, G. A.; Goheen, G. E.
Inorganic Syntheses, 1939 , vol. 1, p. 55 - 59
Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
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Brendan Timmons, R.
Diss. Abstr., Diss. Catholic Univ. of America 1963, S. 1/68 1965 , vol. 26, p. 736
Thomas; Thomas
Transactions of the Faraday Society, 1961 , vol. 57, p. 266
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
Archambault, J. D.; Sisler, H. H.; Ryschkewitsch, G. E.
Journal of Inorganic and Nuclear Chemistry, 1961 , vol. 17, p. 130 - 134
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
in neat (no solvent)
heating N2O4 with SO2Cl2 in bomb tube at 180°C;;
参考文献
Battegay, M.; Denivelle, L.
Bull. Soc. Chim. France (4), 1930 , vol. 47, p. 606 - 612
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
Archambault, J. D.; Sisler, H. H.; Ryschkewitsch, G. E.
Journal of Inorganic and Nuclear Chemistry, 1961 , vol. 17, p. 130 - 134
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Gmelin Handbook: Cl: SVol.B2, 84, page 500 - 502
