in sulfuric acid
Kinetics; in closed reactor, using HCl as gas, at 263-303 K; not isolated, detected by MS, IR, UV in gas phase;
参考文献
Cappa, Christopher D.; Kuipers, Sarah E.; Roberts, Jeanine M.; Gilbert, Abigail S.; Elrod, Matthew J.
Journal of Physical Chemistry A, 2000 , vol. 104, # 19 p. 4449 - 4457
in not given
prepared from KNO2 and POCl3; purified by redistillation in vacuo;
参考文献
Gray, Leslie R.; Higgins, Simon J.; Levason, William; Webster, Michael
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1984 , p. 459 - 468
in neat (no solvent)
slow addn. of dry liquid N2O4 to HSO3Cl; exclusion of moisture; vigorous evolution of NOCl;; pptn.; filtration; dried in vac.;;
参考文献
Jones, C. W. H.; Price, W. J.; Webb, H. W.
Journal of the Chemical Society, 1929 , p. 312 - 315
Full Text Show Details
Gmelin Handbook: S: MVol.B3, 51, page 1641 - 1643