Stoyanovich, F. M.; Marakatkina, M. A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1983 , vol. 19, # 12 p. 1346
Khimiya Geterotsiklicheskikh Soedinenii, 1983 , vol. 19, # 12 p. 1695 - 1697
in diethyl ether inert atm., Schlenk technique; dropwise addn. of thienyl-Li in ether to Zr-complex in ether (-78°C), warmed to room temp. over 12 h; evapn., extn. (CHCl3), filtration, evapn. (red oily residue), washed (pentane), evapn., not further separated; elem. anal.;
Loft, Michael S.; Mowlem, Timothy J.; Widdowson, David A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 2 p. 97 - 104
Dang, Qun; Brown, Brian S.; Liu, Yan; Rydzewski, Robert M.; Robinson, Edward D.; Van Poelje, Paul D.; Reddy, M. Rami; Erion, Mark D.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 9 p. 2880 - 2898
1: thien-2-yl-lithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 3-iodo-pyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591
1: thien-2-yl-lithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 3-bromo-pyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591
1: thien-2-yl-lithium With indium(III) chloride in tetrahydrofuran T=-78 - 20°C; 2: 3-(Trifluoromethylsulfonyloxy)-pyridine With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating; Further stages.;
参考文献
Font-Sanchis, Enrique; Cespedes-Guirao, F. Javier; Sastre-Santos, Angela; Fernandez-Lazaro, Fernando
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3589 - 3591
in diethyl ether; hexane byproducts: cuprous acetate; addn. from a syringe of 2-lithiothiophene soln. to a stirred suspn. of CuI in Et2O, -70°C, (colour change from grey to white then to olive), 2 h, addn. of a soln. of (C4H9)2SnClOAc, stirring 18 h; filtered (Cu(OAc)2), the filtrate vac. concd., elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 430, # 2 p. 149 - 166
