hydrogen; palladium on activated charcoal in ethyl acetate

暂无反应条件数据

pentaphenylferrocenyl di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; 4 h;

1: bromoacetic acid tert-butyl ester With iodine; zinc in tetrahydrofuran T=100°C; 0.0833333 h; microwave irradiation; 2: 1-bromo-4-nitro-benzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=120°C; 0.0833333 h; microwave irradiation; Further stages.;

1: bromoacetic acid tert-butyl ester With zinc in tetrahydrofuran T=20°C; 6 h; Inert atmosphereCooling with ice; 2: 1-chloro-4-nitro-benzene With (1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=70°C; Reformatsky reaction; 12 h; Inert atmosphere;

(1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=20°C; 4 h; Inert atmosphereSealed tube;

1: acetic acid tert-butyl ester With lithium hexamethyldisilazane in toluene T=-78°C; 1 h; Inert atmosphereSealed tube; 2: With zinc(II) chloride in tetrahydrofuran; toluene T=-78°C; 0.5 h; Inert atmosphereSealed tube; 3: 1-bromo-4-nitro-benzene With (1,2,3,4,5-pentaphenylferrocen-1'-yl)-di-tert-butylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; toluene T=20°C; 4 h; Inert atmosphereSealed tube;

N-bromosuccinmide in toluene T=80°C; 1 h;

pyridine; trichlorophosphate in chloroform 5 h;

potassium tert-butylate in ammonia T=-70°C;