1-溴-2-甲基-1-丙烯合成路线 （共 93 条）
参考文献
Chemische Berichte, , vol. 27, p. 1226
参考文献
Zeitschrift fuer Chemie, , p. 524
参考文献
Journal of the Chemical Society, , vol. 105, p. 2295
参考文献
Journal of the Chemical Society, , vol. 105, p. 2295
参考文献
Zhurnal Obshchei Khimii, , vol. 17, p. 971
Chem.Abstr., , p. 4592
反应条件
1: N'-(9H-fluoren-9-ylidene)-4-methylbenzenesulfonohydrazide With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in 1,4-dioxane 0.0166667 h; Inert atmosphere; 2: 1-bromo-2-methyl-1-propene in 1,4-dioxane T=110°C; Inert atmosphere;
参考文献
Barluenga, Jose; Tomas-Gamasa, Maria; Aznar, Fernando; Valdes, Carlos
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3235 - 3240
反应条件
potassium hydroxide; hydrogen; cobalt(II) chloride in water T=45°C; 6 h;
参考文献
Funabiki, Takuzo; Hosomi, Hiroaki; Yoshida, Satohiro; Tarama, Kimio
Journal of the American Chemical Society, 1982 , vol. 104, # 6 p. 1560 - 1568
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=105 - 110°C; 72 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Dyker, Gerald
Angewandte Chemie, 1994 , vol. 106, # 1 p. 117 - 119
反应条件
aluminium trichloride T=25°C; 0.5 h; other alkylation agents, var. time and temp. of reaction, other reagents; Product distributionMechanism;
参考文献
Khalaf, Ali Ali; Albar, Hassan A.
Journal of the Indian Chemical Society, 1995 , vol. 72, # 2 p. 87 - 92
反应条件
1: With sodium iodide; N-methyl-2-(methylamino)ethylamine; copper(l) iodide in sulfolane T=90°C; 23 h; 2: With ammonia in sulfolane; water; pentane
参考文献
MASSACHUSETTS INSTITUTE OF TECHNOLOGY
Patent: WO2004/13094 A2, 2004 ;
Location in patent: Page 59 ;
