2-二氮杂-1-苯乙酮合成路线 （共 259 条）
反应条件
(meso-tetraphenylporphyrin)Ru(CO) in dichloromethane
T=25°C; 24 h; Title compound not separated from byproducts.;
参考文献
Nicolas, Irene; Maux, Paul Le; Simonneaux, Gerard
Tetrahedron Letters, 2008 , vol. 49, # 13 p. 2111 - 2113
参考文献
Hampel; Mueller
Journal fuer Praktische Chemie (Leipzig), 1968 , vol. <4> 38, p. 320,322, 326
反应条件
in acetonitrile
0.0833333 h; Inert atmosphereIrradiation;
参考文献
Allen, Annette D.; Andraos, John; Tidwell, Thomas T.; Vukovic, Sinisa
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 679 - 685
反应条件
sodium azide; cerium(III) chloride in acetonitrile
T=80°C; 5 h;
参考文献
Yadav; Subba Reddy; Srinivas
Chemistry Letters, 2004 , vol. 33, # 7 p. 882 - 883
参考文献
Yates
Journal of the American Chemical Society, 1952 , vol. 74, p. 5376,5380
反应条件
in acetonitrile
0.0833333 h; Inert atmosphereIrradiation;
参考文献
Allen, Annette D.; Andraos, John; Tidwell, Thomas T.; Vukovic, Sinisa
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 679 - 685
参考文献
Erba S.p.A.
Patent: US2892865 , 1957 ;
反应条件
copper(l) iodide; triphenylphosphine in toluene
T=80°C; 16 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Lebel, Helene; Davi, Michael
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 14-15 p. 2352 - 2358
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,2-dichloro-ethane
T=80°C; 8 h;
参考文献
Reddy, B. V. Subba; Reddy, M. Ramana; Rao, Y. Gopal; Yadav; Sridhar
Organic Letters, 2013 , vol. 15, # 3 p. 464 - 467
反应条件
1: 81 percent / diethyl ether
2: 84 percent / SnCl4 / Ambient temperature
View Scheme
参考文献
McKervey, M. Anthony; Ratananukul, Piniti
Tetrahedron Letters, 1983 , vol. 24, # 1 p. 117 - 120
