N-(环己基甲基亚基氨基)-2,4-二硝基苯胺合成路线 （共 10 条）
反应条件
1: aminomethyl-cyclohexane With lithium perchlorate; [3-amino-2,4-dihydroxyphenyl]phenylmethanone in methanol T=20°C; Electrochemical reaction; 2: (2,4-dinitro-phenyl)-hydrazine With sulfuric acid; lithium perchlorate in methanol; ethanol 1 h;
参考文献
Largeron, Martine; Neudorffer, Anne; Fleury, Maurice-Bernard
Angewandte Chemie - International Edition, 2003 , vol. 42, # 9 p. 1026 - 1029
参考文献
Bezier, David; Park, Sehoon; Brookhart, Maurice
Organic Letters, 2013 , vol. 15, # 3 p. 496 - 499
反应条件
1: hydrogenchloride; water / tetrahydrofuran / 3 h / 20 °C / |Glovebox; |Schlenk technique 2: sulfuric acid / ethanol; water / |Glovebox; |Schlenk technique View Scheme
参考文献
Bezier, David; Park, Sehoon; Brookhart, Maurice
Organic Letters, 2013 , vol. 15, # 3 p. 496 - 499
反应条件
1: tris(pentafluorophenyl)-borane / benzene-d6 / 11 h / 23 °C / |Glovebox; |Schlenk technique 2: hydrogenchloride; water / tetrahydrofuran / 3 h / 20 °C / |Glovebox; |Schlenk technique 3: sulfuric acid / ethanol; water / |Glovebox; |Schlenk technique View Scheme
参考文献
Bezier, David; Park, Sehoon; Brookhart, Maurice
Organic Letters, 2013 , vol. 15, # 3 p. 496 - 499
反应条件
1: cyclohexylmethyl alcohol With 1-methyl-1H-imidazole; [Cu(MeCN)]4*CF3SO3; 4,4'-dimethoxy-2,2'-bipyridine; ABNO; oxygen in acetonitrile T=20°C; 1 h; 2: (2,4-dinitro-phenyl)-hydrazine With hydrogenchloride in water; acetonitrile 1 h; Kinetics; Reagent/catalyst;
参考文献
Steves, Janelle E.; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 42 p. 15742 - 15745
反应条件
1: disodium hydrogenphosphate; dichloromethane 2: lithium alanate 3: aqueous H2SO4 View Scheme
参考文献
Jacquier; Fraisse
Bulletin de la Societe Chimique de France, 1957 , p. 108
反应条件
1: lithium alanate 2: aqueous H2SO4 View Scheme
参考文献
Jacquier; Fraisse
Bulletin de la Societe Chimique de France, 1957 , p. 108
反应条件
1: methanol; palladium/calcium carbonate / Hydrogenation View Scheme
参考文献
Heilbron et al.
Journal of the Chemical Society, 1949 , p. 742,743
参考文献
Jacquier; Fraisse
Bulletin de la Societe Chimique de France, 1957 , p. 108
参考文献
Jacquier; Fraisse
Bulletin de la Societe Chimique de France, 1957 , p. 108
Full Text Show Details
Mousseron et al.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 243, p. 1880
