甲基1-氧杂螺[2.5]辛烷-2-羧酸酯合成路线 （共 7 条）
反应条件
[Ni(2,2'-bipyridine)3(2+)][BF4(1-)]2; tetrabutylammomium bromide; zinc dibromide in dichloromethane; N,N-dimethyl-formamide Ambient temperatureelectrolysis (carbon fiber cathode, zinc rod anode);
参考文献
Conan, Annie; Sibille, Soline; Perichon, Jacques
Journal of Organic Chemistry, 1991 , vol. 56, # 6 p. 2018 - 2024
反应条件
sodium methylate in toluene 2 h; 0 deg C to r.t.;
参考文献
Kato, Yasuo
Tetrahedron Letters, 1995 , vol. 36, # 27 p. 4809 - 4812
反应条件
potassium tert-butylate in diethyl ether 20 h; Ambient temperature;
参考文献
Legters, Johan; Thijs, Lambertus; Zwanenburg, Binne
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 1 p. 1 - 15
反应条件
in diethyl ether 20 h; Ambient temperature;
参考文献
Legters, Johan; Thijs, Lambertus; Zwanenburg, Binne
Recueil des Travaux Chimiques des Pays-Bas, 1992 , vol. 111, # 1 p. 1 - 15
参考文献
Aggarwal, Varinder K.; Hebach, Christina
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 8 p. 1419 - 1427
反应条件
1: 94 percent / sodium methoxide / methanol / added water, stand overnight 2: 100 percent / 10percent sulfuric acid / stream of steam under a carbon dioxide atmosphere View Scheme
参考文献
Rodriguez; Benito; Temprano
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 5 p. 1207 - 1210
反应条件
sodium methylate in methanol added water, stand overnight;
参考文献
Rodriguez; Benito; Temprano
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 5 p. 1207 - 1210
