2,3,4,9-四氢-1H-咔唑-1-酮合成路线 （共 50 条）
反应条件
acetic acid in water 5 h; Reflux;
参考文献
Kadam, Sandip A.; Haav, Kristjan; Toom, Lauri; Haljasorg, Toiv; Leito, Ivo
Journal of Organic Chemistry, 2014 , vol. 79, # 6 p. 2501 - 2513
反应条件
1: NaOAc / methanol; H2O 2: CH3COOH; HCl / H2O View Scheme
参考文献
Heterocycles, , vol. 51, # 9 p. 2163 - 2169
反应条件
aluminum tri-bromide; thiophenol 0 deg C, 3 h then 20 deg C, 18 h;
参考文献
Caubere, Catherine; Caubere, Paul; Renard, Pierre; Bizot-Espiart, Jean-Guy; Ianelli, Sandra; et al.
Tetrahedron, 1994 , vol. 50, # 47 p. 13433 - 13448
反应条件
1.1: aq. NaOH / 48 h / 20 °C 1.2: 92 percent / H2O / 0 - 20 °C 2.1: 92 percent / aq. H2SO4 / acetonitrile / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 21 p. 8385 - 8394
反应条件
1.1: aq. NaOH / 48 h / 20 °C 1.2: 92 percent / H2O / 0 - 20 °C 2.1: 92 percent / aq. H2SO4 / acetonitrile / 80 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 21 p. 8385 - 8394
反应条件
acidic medium according to lit. cit. 2, 8; Multistep reaction;
参考文献
Journal of the Indian Chemical Society, , vol. 67, # 1 p. 72 - 73
反应条件
1: 94 percent / MeONa / toluene / 24 h 2: 88 percent / AcONa / H2O; methanol 3: 90 percent / CH3COOH, CF3COOH / 3 h / Heating View Scheme
参考文献
Journal of Chemical Research, Miniprint, , # 9 p. 2001 - 2014
反应条件
sodium hydroxide; oxygen in methanol; water 2 h; also other tetrahydrocarbazol-1-ylidene derivatives; Product distribution;
参考文献
Brunk; Fritz
1985 , vol. 1985, # 9 p. 1715 - 1731
反应条件
1: toluene-4-sulfonic acid / toluene / 2 h / 50 °C / |Inert atmosphere 2: acetic anhydride; bis-[(trifluoroacetoxy)iodo]benzene / 0.17 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 70, # 17 p. 2753 - 2760
反应条件
acetic acid Fischer Indole Synthesis; 40 h; Reflux; Overall yield = 97.9percent;
参考文献
Journal of Organic Chemistry, , vol. 78, # 16 p. 7796 - 7808
