2,2,8,8-四甲基-3,6-壬二烯-5-酮合成路线 （共 11 条）
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 24 h; Molecular sieveInert atmosphere;
参考文献
Chalifoux, Wesley A.; McDonald, Robert; Ferguson, Michael J.; Tykwinski, Rik R.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 42 p. 7915 - 7919
反应条件
chromium(VI) oxide; acetic acid
参考文献
Sparks; Marvel
Journal of the American Chemical Society, 1936 , vol. 58, p. 865,867
反应条件
1: diluted ethanol; HCl / 0 °C 2: CrO3; glacial acetic acid View Scheme
参考文献
Sparks; Marvel
Journal of the American Chemical Society, 1936 , vol. 58, p. 865,867
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.25 h / 0 °C / |Inert atmosphere 1.2: 2.08 h / 0 - 20 °C / |Inert atmosphere 2.1: manganese(IV) oxide / dichloromethane / 20 °C View Scheme
参考文献
Qiu, Yi-Feng; Yang, Fang; Qiu, Zi-Hang; Zhong, Mei-Jin; Wang, Li-Jing; Ye, Yu-Ying; Song, Bo; Liang, Yong-Min
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12018 - 12028
参考文献
Ivitzky
Bulletin de la Societe Chimique de France, 1924 , vol. <4>35, p. 357
参考文献
Sparks; Marvel
Journal of the American Chemical Society, 1936 , vol. 58, p. 865,867
参考文献
Sparks; Marvel
Journal of the American Chemical Society, 1936 , vol. 58, p. 865,867
参考文献
Ivitzky
Bulletin de la Societe Chimique de France, 1924 , vol. <4>35, p. 357
反应条件
sodium borohydride; hydrogen sulfide in ethanol; water; sodium ethanolate
参考文献
Detty, Michael Ray; Virkler, Peter Robert
Patent: US2002/22723 A1, 2002 ;
反应条件
sodium sulfide; sodium ethanolate in ethanol
Ambient temperature;
参考文献
Detty, Michael R.; Hassett, James W.; Murray, Bruce J.; Reynolds, George A.
Tetrahedron, 1985 , vol. 41, # 21 p. 4853 - 4860
