(R)-(+)-N-乙酰基-甲基苄胺合成路线 (共 87 条)
反应条件
molecular sieve; lipase B from Candida antarctica in 1,4-dioxane T=30°C; aminolysis; Enzymatic reaction;
参考文献
Tetrahedron Asymmetry, , vol. 11, # 7 p. 1459 - 1463
反应条件
Candida antarctica (Novozym 435) T=21°C; 504 h; Enzymatic reaction;
参考文献
Davis; Durden
Synthetic Communications, 2001 , vol. 31, # 4 p. 569 - 578
反应条件
1: H2NOSO3H / tetrahydrofuran / 10 h 2: 1,1'-carbonyldiimidazole / toluene View Scheme
参考文献
Chemistry - A European Journal, , vol. 6, # 10 p. 1840 - 1846
反应条件
Candida antarctica lipase B; C70H58O14Ru2; sodium carbonate in toluene T=90°C; 72 h; optical yield given as percent ee;
参考文献
Beilstein Journal of Organic Chemistry, , vol. 6, p. 823 - 829
反应条件
triethylamine in tetrahydrofuran T=20°C; 10 h;
参考文献
Tetrahedron Asymmetry, , vol. 19, # 14 p. 1641 - 1646
反应条件
Candida antarctica lipase B immobilized on acrylic resin in toluene T=25°C; 0.0666667 h; Resolution of racemateFlow reactor; TemperatureTime;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 20 p. 3332 - 3336
反应条件
1,1'-carbonyldiimidazole in toluene Acetylation; Title compound not separated from byproducts;
参考文献
Chemistry - A European Journal, , vol. 6, # 10 p. 1840 - 1846
反应条件
2,2'-azo-bisisobutyronitrile; triphenylstannane in benzene reductive deselenenylation; 3 h; Heating;
参考文献
European Journal of Organic Chemistry, , # 20 p. 3451 - 3457
反应条件
Aliquatreg; 336 in tetrahydrofuran T=20°C; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Journal of the American Chemical Society, , vol. 127, # 17 p. 6138 - 6139
反应条件
triethylamine in diethyl ether; N-dodecane; dichloromethane; toluene
参考文献
Chemistry - A European Journal, , vol. 15, # 46 p. 12780 - 12790