(9ci)-2-环己基-1H-苯并咪唑合成路线 （共 17 条）
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide in neat (no solvent)
T=50°C; 18 h; Green chemistry;
参考文献
Barbero, Margherita; Cadamuro, Silvano; Dughera, Stefano
Arkivoc, 2012 , vol. 2012, # 9 p. 262 - 279
反应条件
1: 98 percent / AlCl3
2: 95 percent / (diacetoxyiodo)benzene / toluene / 110 °C
View Scheme
参考文献
Ramsden, Christopher A.; Rose, Helen L.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2319 - 2327
反应条件
1: 98 percent / AlCl3
2: 95 percent / (diacetoxyiodo)benzene / toluene / 110 °C
View Scheme
参考文献
Ramsden, Christopher A.; Rose, Helen L.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 16 p. 2319 - 2327
反应条件
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 20 °C
2: 2-iodosylbenzoic acid / dimethyl sulfoxide / 5 h / 25 °C
View Scheme
参考文献
Moorthy, Jarugu Narasimha; Neogi, Ishita
Tetrahedron Letters, 2011 , vol. 52, # 30 p. 3868 - 3871
反应条件
1: |Inert atmosphere
2: PIDA; caesium carbonate / 2,2,2-trifluoroethanol / 1.5 h / 25 °C
View Scheme
参考文献
Huang, Jinbo; He, Yimiao; Wang, Yong; Zhu, Qiang
Chemistry - A European Journal, 2012 , vol. 18, # 44 p. 13964 - 13967
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 20 °C
2: 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical / N,N-dimethyl-formamide / 5 h / 110 °C
View Scheme
参考文献
Xue, Ding; Long, Ya-Qiu
Journal of Organic Chemistry, 2014 , vol. 79, # 10 p. 4727 - 4734
参考文献
Jerchel et al.
Justus Liebigs Annalen der Chemie, 1952 , vol. 575, p. 162,167
