in ethanol; water
soln. of Ni salt in H2O heated to 60-70°C; soln. of ligand in EtOH added over 30 min; stirred at 60-70°C for 2 h; evapd. by 2/3 of initial vol.; cooled to room temp.; stored for 2 d; ppt. collected by filtration; detd. by elem. anal., gravimetric analysis and X-ray diffraction;
参考文献
Sadigova; Magerramov; Allakhverdiev; Alieva; Chyragov; Vekilova
Russian Journal of General Chemistry, 2003 , vol. 73, # 12 p. 1932 - 1935
Burges, W. M.; Eastes, J. W.
Journal of the American Chemical Society, 1941 , vol. 63, p. 2674 - 2676
Full Text View citing articles Show Details
Gmelin Handbook: Ni: MVol.AI, 10.3, page 616 - 621
Burges, W. M.; Eastes, J. W.
Journal of the American Chemical Society, 1941 , vol. 63, p. 2674 - 2676
Full Text View citing articles Show Details
Gmelin Handbook: Ni: MVol.AI, 10.3, page 616 - 621
