2-氯-2,4,6-环庚三烯-1-酮合成路线 (共 41 条)
参考文献
ter Borg,A.P. et al.
Recueil des Travaux Chimiques des Pays-Bas, 1962 , vol. 81, p. 177 - 184
参考文献
Doering; Knox
Journal of the American Chemical Society, 1952 , vol. 74, p. 5683,5686
Full Text Show Details
Abadir et al.
Journal of the Chemical Society, 1952 , p. 2350,2351
参考文献
Doering; Knox
Journal of the American Chemical Society, 1952 , vol. 74, p. 5683,5686
Full Text Show Details
Abadir et al.
Journal of the Chemical Society, 1952 , p. 2350,2351
反应条件
2: platinum; ethanol / Hydrogenation
View Scheme
参考文献
Doering,von E.; Hiskey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5688,5693
反应条件
bis-triphenylphosphine-palladium(II) chloride; caesium carbonate in tetrahydrofuran; water
T=75°C; Suzuki Coupling; 16 h; Inert atmosphere;
参考文献
UNIVERSITY OF CONNECTICUT; WRIGHT, Dennis L.; ANDERSON, Amy C.; VAN HEYST, Michael; ONONYE, Sophia
Patent: WO2013/192554 A1, 2013 ;
Location in patent: Page/Page column 15 ;
参考文献
Doering,von E.; Hiskey
Journal of the American Chemical Society, 1952 , vol. 74, p. 5688,5693
参考文献
Abadir et al.
Journal of the Chemical Society, 1952 , p. 2350,2351
反应条件
hydrazine hydrate in methanol
Heating;
参考文献
Imafuku,K. et al.
Bulletin of the Chemical Society of Japan, 1979 , vol. 52, # 8 p. 2447 - 2448
反应条件
1.) benzene, Et2O, -78 deg C, 20 min, 2.) 78 deg C -> 0 deg C; Yield given. Multistep reaction;
参考文献
Cavazza, Marino; Morganti, Gioia; Guerriero, Antonio; Pietra, Francesco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 199 - 202
反应条件
1.) benzene, Et2O, -78 deg C, 30 min, 2.) 0 deg C, overnight; Yield given. Multistep reaction;
参考文献
Cavazza, Marino; Morganti, Gioia; Guerriero, Antonio; Pietra, Francesco
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 2 p. 199 - 202