in chloroform; water aq. soln. of Cu(NO3)2 combined with CHCl3; sodium octanoate added; not isolated;

in not given 50-55°C; product was washed with water and alcohol, dried at 100-105°C under reduced pressure, and recrystd. from hot benzene; elem. anal.;

in water required amt. of Cu-salt and Na-carboxylate were reacted; recrystn. from MeOH;

in water precipitate;;

in acetone Electrolysis; 5 h, initial voltage 50 V; solvent reduced to 50percent, solid was collected, washed with acetonitrile, dried in vacuo dfor 3-4 h at room temp.; elem.anal;

in chloroform; water two-phase react.; Cu(OAc)2 in a min. vol. of H2O mixed with the same vol. of CHCl3; stoich. quantity of octanoic acid added dropwise with stirring; a green-blue color developed slowly in the CHCl3 layer; CHCl3 layer was sepd. from the almost colorless aq. layer; CHCl3 soln. rotatory evapd.; residue washed (H2O) and twice recrystd. (MeOH); elem. anal.;