1,1,7-三氯-1-庚烯合成路线 （共 12 条）
反应条件
dihydrogen peroxide; ozone 1) glacial acetic acid, 5-8 deg C, 10 h, 2) 4 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Zakharkin, L. I.; Zhigareva, G. G.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1831 - 1833
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2051 - 2054
反应条件
iron(III) chloride
T=45 - 55°C;
参考文献
Nesmejanow; Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1953 , p. 988,989;engl.Ausg.S.879
反应条件
pentacarbonyliron(0); butane-1-thiol
T=140°C; 4 h; further tetrachloroalkanes; further metal carbonyl, other periods of time; Product distribution;
参考文献
Petrova, R. G.; Churkina, T. D.; Golikova, I. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 8 p. 1642 - 1646
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 8 p. 1816 - 1820
参考文献
du Pont de Nemours and Co.
Patent: US2410541 , 1942 ;
参考文献
Nesmejanow; Semenow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1959 , p. 2119; engl. Ausg. S. 2022
反应条件
perchloric acid
T=130°C;
参考文献
Freidlina; Wasil'ewa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 35;engl.Ausg.S.32
参考文献
Freidlina; Wasil'ewa
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 35;engl.Ausg.S.32
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
反应条件
1: ethanol
2: sodium; diethyl ether
View Scheme
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
反应条件
1: methanol / 115 °C
2: diethyl ether; sodium
View Scheme
参考文献
Sacharkin
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 1009,1013
Chem.Abstr., 1956 , # 1121
