3-溴-2,2-二甲基-1-丙醇合成路线 (共 29 条)
反应条件
1: sodium 2: ueber Messingspaene bei Rotglut View Scheme
参考文献
Franke; Hinterberger
Monatshefte fuer Chemie, 1922 , vol. 43, p. 658
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
反应条件
1: sodium amalgam; water; methanol 2: chromic acid View Scheme
参考文献
Franke
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1904
反应条件
T=64 - 109°C; Kinetics;
参考文献
Journal of the American Chemical Society, , vol. 78, p. 1699,1700
反应条件
1: aq. NaN3 2: H2 / Pt-C / ethanol View Scheme
参考文献
Alewood,P.F. et al.
Canadian Journal of Chemistry, 1974 , vol. 52, p. 4083 - 4089
反应条件
potassium hydroxide in ethylene glycol T=60°C; 1 h; Heating;
参考文献
Dale, Johannes; Fredriksen, Siw B.
Acta Chemica Scandinavica, 1991 , vol. 45, # 1 p. 82 - 91
参考文献
Searles; Gortatowski
Journal of the American Chemical Society, 1953 , vol. 75, p. 3030
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Searles et al.
Journal of Organic Chemistry, 1959 , vol. 24, p. 1839,1842
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; 18 h;
参考文献
Meiresonne, Tamara; Mangelinckx, Sven; De Kimpe, Norbert
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 7085 - 7091
反应条件
pyridinium chlorochromate in dichloromethane T=20°C; Oxidation; cyclization; trimerization; 7 h; Product distribution; Further Variations:Reagents;
参考文献
Jauch
Advanced Synthesis and Catalysis, 2000 , vol. 342, # 1 p. 100 - 101
反应条件
methanol; sodium iodide T=170°C;
参考文献
Zhurnal Obshchei Khimii, , vol. 16, p. 751,759
Chem.Abstr., , p. 2033