2-羟基-1,2,2-三苯乙酮合成路线 （共 78 条）
反应条件
in tetrahydrofuran
T=-78°C; var. solv. and temp.: var. ratio of product, the radical intermediers (UV, EPR, 13C NMR); Product distributionMechanismKinetics;
参考文献
Nudelman, N. Sbarbati; Doctorovich, Fabio
Tetrahedron, 1994 , vol. 50, # 16 p. 4651 - 4666
反应条件
ammonium chloride
1.) THF, room temperature, 2.) 150 deg C, 1 min; Multistep reaction;
参考文献
Holm, T.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1987 , vol. 41, # 4 p. 278 - 284
反应条件
in acetone
Product distribution;
参考文献
Shadrina, L. P.; Dormidontov, Yu. P.; Ponomarev, V. G.; Lapkin, I. I.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1987 , vol. 23, # 9 p. 964 - 967
Khimiya Geterotsiklicheskikh Soedinenii, 1987 , # 9 p. 1206 - 1209
参考文献
Stevens; DeYoung
Journal of the American Chemical Society, 1954 , vol. 76, p. 718
参考文献
Werner
Chemische Berichte, 1906 , vol. 39, p. 1287
参考文献
Gardeur
Chem. Zentralbl., 1897 , vol. 68, # II p. 661
参考文献
Finger; Gaul
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 111, p. 58
参考文献
Biltz
Chemische Berichte, 1899 , vol. 32, p. 655
参考文献
Finger; Gaul
Journal fuer Praktische Chemie (Leipzig), 1925 , vol. <2> 111, p. 58
反应条件
1: pyridine; thionyl chloride / 0 °C
2: sodium hydrogencarbonate / acetone / -60 °C
3: chloroform-d1 / 0.67 h / |Photolysis
View Scheme
参考文献
Jang, Sukjin; Chowdhury, Azhad; Kang, Jeonghee; Lee, Jong I.
Letters in Organic Chemistry, 2014 , vol. 11, # 3 p. 230 - 235
