(3,3-二甲基-1-丁炔)-苯合成路线 （共 61 条）
反应条件
silica gel; phosphorus(III) iodide in dichloromethane 0.3 h; various reaction times and adsorbent; Product distribution;
参考文献
Kropp, Paul J.; Crawford, Scott D.
Journal of Organic Chemistry, 1994 , vol. 59, # 11 p. 3102 - 3112
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; triethylamine in tetrahydrofuran
T=20°C; 0.0833333 h;
2: With copper(l) iodide
T=20°C; 24 h;
参考文献
Dooley, Johnathon D.; Reddy Chidipudi, Suresh; Lam, Hon Wai
Journal of the American Chemical Society, 2013 , vol. 135, # 29 p. 10829 - 10836
反应条件
potassium fluoride; 18-crown-6 ether in tetrahydrofuran
T=20°C; 8 h;
参考文献
Jayanth, Thiruvellore Thatai; Jeganmohan, Masilamani; Cheng, Mu-Jeng; Chu, San-Van; Cheng, Chien-Hong
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2232 - 2233
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran; pentane
T=25°C; 2 h; Inert atmosphere;
参考文献
Truong, Thanh; Daugulis, Olafs
Organic Letters, 2011 , vol. 13, # 16 p. 4172 - 4175
反应条件
PhCCI in dimethyl sulfoxide
Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (275-W sunlamp, 35-40°C, 7h);; mixt. poured into water; extn. with benzene; ext. washed (aq. Na2S2O3), dried (Na2SO4) and concd. (vacuum); yield detd. by GLC;;
参考文献
Russell, Glen A.; Ngoviwatchai, Preecha; Tashtoush, Hasan I.; Pla-Dalmau, Anna; Khanna, Rajive K.
Journal of the American Chemical Society, 1988 , vol. 110, # 11 p. 3530 - 3538
反应条件
aluminium trichloride in dichloromethane
T=-78°C; 6 h;
参考文献
Capozzi, Giuseppe; Romeo, Giovanni; Marcuzzi, Franco
Journal of the Chemical Society, Chemical Communications, 1982 , # 16 p. 959 - 960
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Capozzi, Giuseppe; Ottana, Rosaria; Romeo, Giovanni; Marcuzzi, Franco
Gazzetta Chimica Italiana, 1985 , vol. 115, # 6 p. 311 - 314
反应条件
sodium iodide in dimethyl sulfoxide
T=35 - 40°C; 2 h; Irradiation;
参考文献
Russell, Glen A.; Baik, Woonphil; Ngoviwatchai, Preecha; Kim, Byeong Hyo
Acta Chemica Scandinavica, 1990 , vol. 44, # 2 p. 170 - 177
反应条件
copper(l) iodide; potassium carbonate in ethylene glycol dimethyl ether; N,N-dimethyl-formamide
T=20°C; 1 h;
参考文献
Yu, Chan-Mo; Kweon, Jae-Hong; Ho, Pil-Su; Kang, Sin-Cheol; Lee, Gong Yeal
Synlett, 2005 , # 17 art. no. U23005ST, p. 2631 - 2634
反应条件
dipotassium peroxodisulfate; copper; silver nitrate in water; acetonitrile
T=110°C; 12 h;
参考文献
Mai, Wen-Peng; Song, Ge; Sun, Gang-Chun; Yang, Liang-Ru; Yuan, Jin-Wei; Xiao, Yong-Mei; Mao, Pu; Qu, Ling-Bo
RSC Advances, 2013 , vol. 3, # 42 p. 19264 - 19267
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=22°C; 3 h;
参考文献
Negishi, Ei-ichi; Akiyoshi, Kazunari; Takahashi, Tamotsu
Journal of the Chemical Society, Chemical Communications, 1987 , # 6 p. 477 - 478
