3-苯基丙-2-烯-1-醇合成路线 （共 318 条）
参考文献
Jurd,L. et al.
Tetrahedron, 1973 , vol. 29, p. 2347 - 2353
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Jurd; Stevens; King Jr.; Mihara
Journal of pharmaceutical sciences, 1971 , vol. 60, # 11 p. 1753 - 1755
反应条件
1: tBuOOH; L-(+)-diethyl tartrate; Ti(OiPr)4 / CH2Cl2 / -20 °C 2: Red-Al / 1,2-dimethoxy-ethane View Scheme
参考文献
McNeill; Thomas
Synthesis, 1994 , # 3 p. 322 - 334
反应条件
titanium(IV) isopropylate; manganese(IV) oxide; 1-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene in tetrahydrofuran oxidation-Wittig reaction; 48 h; Heating;
参考文献
Synlett, , # 2 p. 215 - 218
反应条件
potassium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in tetrahydrofuran T=20°C; 12 h;
参考文献
Tetrahedron, , vol. 63, # 51 p. 12695 - 12701
反应条件
potassium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene T=20°C; 12 h;
参考文献
Kiyooka, Syun-ichi; Wada, Yosuke; Ueno, Mahuyu; Yokoyama, Takeshi; Yokoyama, Reiko
Tetrahedron, 2007 , vol. 63, # 51 p. 12695 - 12701
反应条件
NOBF4 in pyridine T=0°C; 1 h; Inert atmosphereSchlenk technique; Overall yield = 47percent; Overall yield = 91 mg; regioselective reaction;
参考文献
Matsubara, Ryosuke; Saeki, Yuta; Li, Jianhua; Eda, Kazuo
Synthesis (Germany), 2013 , vol. 45, # 11 art. no. SS-2013-F0183-OP, p. 1524 - 1528
反应条件
polymethylhydrosiloxane; iodine in chloroform T=20°C; 0.416667 h;
参考文献
Chemistry Letters, , vol. 36, # 6 p. 800 - 801
反应条件
diiodo monosilane in chloroform-d1 T=22°C;
参考文献
Journal of Organic Chemistry, , vol. 55, # 9 p. 2927 - 2938
反应条件
trimethylsilyl iodide in chloroform-d1 T=22°C; or with diiodosilane (DIS) instead of TMSI;
参考文献
Journal of Organic Chemistry, , vol. 55, # 9 p. 2927 - 2938
反应条件
1.1: (+)-diethyl tartrate; Ti(O-i-Pr)4; tert-butylhydroperoxide 1.2: triethylamine; 4-(dimethylamino)pyridine 1.3: p-toluenesulfonic acid / tetrahydrofuran; H2O 2.1: p-toluenesulfonic acid / acetone / 20 °C 3.1: tetrabutylammonium fluoride / tetrahydrofuran / 20 °C View Scheme
参考文献
Nakashima, Katsuyuki; Kikuchi, Naoki; Shirayama, Daisuke; Miki, Takuo; Ando, Kazuhiro; Sono, Masakazu; Suzuki, Shinya; Kawase, Masaki; Kondoh, Masuo; Sato, Masao; Tori, Motoo
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 2 p. 387 - 394
