N,N-二甲基-1-(2-甲基苯基)甲胺合成路线 (共 30 条)
反应条件
1: With titanium(IV) isopropylate; triethylamine in ethanol
T=25°C; 12 h;
2: With sodium tetrahydroborate in ethanol
T=25°C; 12 h;
参考文献
Li, Hu; Cai, Gui-Xin; Shi, Zhang-Jie
Dalton Transactions, 2010 , vol. 39, # 43 p. 10442 - 10446
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; cesium fluoride
24 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Shirai, Naohiro; Watanabe, Yoko; Sato, Yoshiro
Journal of Organic Chemistry, 1990 , vol. 55, # 9 p. 2767 - 2770
反应条件
sodium amide in ammonia
T=-40 - -35°C; 4 h;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617
反应条件
sodium amide in ammonia
T=-40 - -35°C; 4 h;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617
反应条件
sodium amide in ammonia
T=-40 - -35°C; 4 h;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617
反应条件
potassium hydroxide in N,N-dimethyl-formamide
T=35 - 40°C;
参考文献
Kocharyan, S. T.; Karapetyan, V. E.; Razina, T. L.; Babayan, A. T.
J. Gen. Chem. USSR (Engl. Transl.), 1990 , vol. <2> 60, # 11 p. 2543 - 2549,2277 - 2282
参考文献
Knabe,J.; Shukla,U.R.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1962 , vol. 295, p. 690 - 697
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
10 h; Heating; Further byproducts given;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
10 h; Heating; Further byproducts given;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
10 h; Heating; Further byproducts given;
参考文献
Sato, Yoshiro; Yagi, Yoko; Koto, Masami
Journal of Organic Chemistry, 1980 , vol. 45, # 4 p. 613 - 617