反应条件
1: 1.) n-BuLi / 1.) THF, hexane, a) 0 deg C, 30 min, b) reflux, 90 min, 2.) THF, hexane, reflux, 90 min
2: 300 mg / BBr3 / CH2Cl2 / 1.) 0 deg C, 45 min, 2.) RT, 4 h
View Scheme
参考文献
Groweiss, Amiram; Cardellina II, John H.; Pannell, Lewis K.; Uyakul, Duangchan; Kashman, Yoel; Boyd, Michael R.
Journal of Natural Products, 1997 , vol. 60, # 2 p. 116 - 121