2-苯基-4-五亚乙基六胺-2-醇合成路线 (共 59 条)
反应条件
Chromium (III) chloride; acetophenone in tetrahydrofuran; diethyl ether -70 to 20 deg C in 14 h, further reagents: MnCl2; Product distribution;
参考文献
Kauffmann, Thomas; Bonrath, Werner; Beirich, Christoph; Li, Weichang; Pahde, Claudia; et al.
Chemische Berichte, 1993 , vol. 126, # 9 p. 2093 - 2100
反应条件
Chromium (III) chloride; ccyclohexanonecarbaldehyde in tetrahydrofuran; diethyl ether -70 to 20 deg c in 14 h, further reagents: MnCl2; Product distribution;
参考文献
Kauffmann, Thomas; Bonrath, Werner; Beirich, Christoph; Li, Weichang; Pahde, Claudia; et al.
Chemische Berichte, 1993 , vol. 126, # 9 p. 2093 - 2100
反应条件
CoCl2 in tetrahydrofuran Ambient temperatureother transition-metal-catalyst; Product distribution;
参考文献
Araki, Shuki; Ohmura, Masayuki; Butsugan, Yasuo
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 5 p. 1607 - 1608
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; ethylene,methyl acetate; carbon monoxide in tetrahydrofuran
参考文献
Kondo, Teruyuki; Kodoi, Kouichi; Nishinaga, Eiji; Okada, Takumi; Morisaki, Yasuhiro; Watanabe, Yoshihisa; Mitsudo, Take-Aki
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5587 - 5588
反应条件
Ru(2 wt)/CeO2 in 1,3,5-trimethyl-benzene T=170°C; 24 h; Inert atmosphere;
参考文献
Miura, Hiroki; Wada, Kenji; Hosokawa, Saburo; Sai, Masahiro; Kondo, Teruyuki; Inoue, Masashi
Chemical Communications, 2009 , # 27 p. 4112 - 4114
反应条件
cobalt(II) chloride in acetonitrile T=45°C; 7 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
acetic anhydride; cobalt(II) chloride in acetonitrile T=45°C; 7 h;
参考文献
Iqbal, Javed; Srivastava, Rajiv Ranjan
Journal of Organic Chemistry, 1992 , vol. 57, # 7 p. 2001 - 2007
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; ethylene,methyl acetate; carbon monoxide in tetrahydrofuran
参考文献
Kondo, Teruyuki; Kodoi, Kouichi; Nishinaga, Eiji; Okada, Takumi; Morisaki, Yasuhiro; Watanabe, Yoshihisa; Mitsudo, Take-Aki
Journal of the American Chemical Society, 1998 , vol. 120, # 22 p. 5587 - 5588
反应条件
sodium hydride in tetrahydrofuran T=65°C; Etherification; 1 h;
参考文献
Schmidt, Bernd; Wildemann, Holger
European Journal of Organic Chemistry, 2000 , # 18 p. 3145 - 3163